Synthesis, Characterization and Biological Activity of New Amides Containing Azo Moieties
Elham Abdalrahem Bin Selim, Mohammed Hadi Al–Douh, Samia Mabrook Bin Mahram, Wedad Mohammed Al–Haik, Khalid Saeed Sonbol
Asian Journal of Applied Chemistry Research · pp. 11–22 · Published 15 Feb 2022
10.9734/ajacr/2022/v11i230250Abstract
Three new amide compounds 6, 8 and 9 were derived from diazo dye 4. 4-Hydroxy-3-methoxy-5-(2,6-dinitrophenyl) benzaldehyde 4 was reacted separately with compounds 5 and 7 to obtain 6 and 8, respectively. The amide compound 9 was synthesized by two different methods. The reaction between 6 and a diacyl chloride compound 7 gave compound 9. Also, compound 9 was produced via the reaction of compound 8 and an N-terminus compound 5. All compounds were characterized by their melting points, UV-Vis, and FTIR spectra. Moreover, the mass spectrum and elemental analysis of compound 9 were determined. All three synthesized compounds were tested against P. mirabilis, E. coli, and S. aureus at different concentrations and showed significant results.
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