Skip to content
Research Article Open access CC BY 4.0

An Investigation on Synthesis of Silver Nanoparticles

Md. Ashraful Alam, Salma Akter Munni, Sabrina Mostafa, Raton Kumar Bishwas, Shirin Akter Jahan

Asian Journal of Research in Biochemistry · pp. 1–10 · Published 4 May 2023

10.9734/ajrb/2023/v12i3234

Abstract

Introduction: Nano science and nano biotechnology provided enormous opportunities for exploring the bactericidal and fungicidal activities. Since ancient times, silver was known for its anti-bacterial effects and for centuries it has been used for prevention and control of disparate infections. On the effective use silver nanomaterials synthesized and characterized play a vital role of the modern science. Aims: Our goal is to prepare silver nanomaterials since studies have shown that silver nanoparticles have efficient activity against bacterial biofilms. Methodology: The silver nanoparticles were generally synthesized by non-aqueous sol-gel technique in the presence of different precursor by chelating agent. Results: Here found a cubic unit cell with miller indices (111) (200) (220) (311) (222) and crystallite size around 50.00nm by XRD. The morphology of the prepared nano particles has been revealed by SEM below 10.00 nm and TEM is below 5.00nm in size of graphical presentation such as size, shape, surface etc. of the nanoparticles. DLS is a unique technique to discern particle size around 65.00nm and size distributions in aqueous or physiological solutions of the nanoparticles. Conclusion: The studies on the combined synthesized and use of AgNPs with other antimicrobial agents generally help reduce the problem of toxicity and to avoid the potential for development of resistance and strongly enhance the microbicidal effect. This paper describes a short and very precise description about the chemical synthesis process of silver nanoparticles like no aqueous SGM. Also, this paper contains a brief description about different characterization technique of nanoparticles like X-ray Diffraction review the shape of crystal a cubic unit cell with miller indices (111) (200) (220) (311) (222) where crystallite size around 50.00nm, the morphology of the prepared nanoparticles has been revealed with size 10.00nm by SEM, Dynamic Light Scattering discern particle size around 65.00nm and Transmission Electron Microscope review the spherical shape of the nanomaterials.  Further investigation will be continuing the antimicrobial activity test of AgNPs with ceramic coating.

Cell destruction (CD) silver nanoparticles (AgNPs) sol-gel method (SGM) TEM analysis (TA) XRD technique (XRDT)

Cited by 10

Study of sol-gel derived silver nanoparticle (AgNPs): X-ray computed crystal growth mechanism and thermal analysis

Md. Ashraful Alam, Raton Kumar Bishwas, Sabrina Mostofa · South African Journal of Chemical Engineering · 2026

Crystallographic phase stability of nanocrystalline polymorphs TiO2 by tailoring hydrolysis pH

Md. Ashraful Alam, Raton Kumar Bishwas, Sabrina Mostofa · South African Journal of Chemical Engineering · 2024

Crystallinity integration and crystal growth behavior study of preferred oriented (111) cubic silver nanocrystal

Md. Ashraful Alam, Sumaiya Islam Sadia, Md. Khalid Hossain Shishir · Inorganic Chemistry Communications · 2025

Stoichiometry crystallographic phase analysis and crystallinity integration of silver nanoparticles: A Rietveld refinement study

Md. Rafayet Al-Mahmud, Md. Khalid Hossain Shishir, Shanawaz Ahmed · Journal of Crystal Growth · 2024

Synthesis and crystallinity integration of copper nanoparticles by reaction medium

Mobashsara Tabassum, Md. Ashraful Alam, Sabrina Mostofa · Journal of Crystal Growth · 2024

A comprehensive review on the biomass-mediated synthesis of silver nanoparticles: Opportunities and challenges

Dinesh Kumar, Sunil Kumar, Amol D. Gholap · Journal of Environmental Chemical Engineering · 2025

Crystallinity integration of anatase (TiO2) nanocrystal by whole powder pattern fitting (WPPF) method: A Rietveld refinement study

Shanawaz Ahmed, Md. Khalid Hossain Shishir, Md. Tarikul Islam · Results in Materials · 2025

Article metrics

Real usage data collected on this platform.

0

Page views

0

PDF downloads

0

Outbound clicks

10

Citations

Views by country

Approximate, from request IP at view time — not citizenship or institution. Countries with fewer than 5 views are grouped as "Other".

No views recorded yet.

Traffic sources

Referring site, by host.

No traffic recorded yet.

Views and downloads exclude known bots/crawlers. Citations combines this platform's own DOI-resolved index with each external source's own reported total — see Cited by above for individually listed citing works. Last refreshed 0 seconds ago.