Synthesis, Characterization, Thermal Analysis and Antibacterial Activity of Cu (II) and Ni(II) Complexes with Thiosemicarbazone Derived from  Thiophene-2-aldehyde

Dipta Sarker; Md. Faruk Hossen; Md. Kudrat-E-Zahan; Md. Masuqul Haque; Rausan Zamir; Md. Ali Asraf

Research Article Open access CC BY 4.0

Synthesis, Characterization, Thermal Analysis and Antibacterial Activity of Cu (II) and Ni(II) Complexes with Thiosemicarbazone Derived from Thiophene-2-aldehyde

Dipta Sarker, Md. Faruk Hossen, Md. Kudrat-E-Zahan, Md. Masuqul Haque, Rausan Zamir, Md. Ali Asraf

Journal of Materials Science Research and Reviews · pp. 64–74 · Published 25 Apr 2020

Abstract

Metal complexes have been synthesized by the reaction of thiophene-2- aldehyde thiosemicarbazone with Cu(OAc)2 and Ni(OAc)2. The thiosemicarbazone coordinates to metal ions through the thionic sulfur and the azomethine nitrogen. The thiosemicarbazone is obtained by the reaction of thiosemicarbazide with thiophene-2- aldehyde. The identities of these compounds have been elucidated by IR and ESI-MS spectroscopic methods and elemental analyses. Thermogravimetric analysis data indicates that the metal complexes are thermally stable. The antibacterial activity of the synthesized compounds are tested by the disc diffusion assay against Gram-positive and Gram-negative bacteria. The antibacterial screening activity revealed that complexes showed moderate activity against tested bacterial strains and slightly higher compared to the ligand, L.

Thiosemicarbazone complexation thermal analysis antibacterial activity.

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Dipta Sarker, Md. Faruk Hossen, Md. Kudrat-E-Zahan, Md. Masuqul Haque, Rausan Zamir, Md. Ali Asraf (2020). Synthesis, Characterization, Thermal Analysis and Antibacterial Activity of Cu (II) and Ni(II) Complexes with Thiosemicarbazone Derived from Thiophene-2-aldehyde. Journal of Materials Science Research and Reviews , 64–74.

Affiliations

Dipta Sarker — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.
Md. Faruk Hossen — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.
Md. Kudrat-E-Zahan — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.
Md. Masuqul Haque — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.
Rausan Zamir — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.
Md. Ali Asraf — Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh.

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