Synthesis, Chracterization and Antibacterial Activity of Cd(II) and Zr(IV) Peroxo-complexes
Md. Mahasin Ali, Md. Nur Amin Bitu, Md. Saddam Hossain, Md. Faruk Hossen, Md. Ali Asraf, Md. Akhter Farooque, Md. Kudrat-E- Zahan
Asian Journal of Chemical Sciences · pp. 22–28 · Published 3 Jul 2020
10.9734/ajocs/2020/v8i119033Abstract
Two new peroxo-complexes of Cd(II) and Zr(IV) ion containing Schiff base (SB) were synthesized and characterized by Thin Layer Chromatography (TLC), Elemental analyses, conductivity, magnetic moment measurements, UV-Vis. and FT-IR spectral studies. The Schiff base ligand derived from cinnamaldehyde and o-aminophenol participated in complexation through a single pot reaction. FT-IR spectra showed that the Schiff base ligand coordinated to the metal ion through nitrogen of azomethine group and oxygen of hydroxyl group & peroxo group (O-O). The molar conductance values indicated the non-electrolytic nature of both the complexes. Antibacterial activity of the complexes was tested against four pathogenic bacteria, two Gram-positive Staphylococcus aureus & Bacillus cereus and two Gram-negative Escherichia coli & Shigella dysenteriae with standard Kanamycin-30. The result showed that Cd(II) complex exhibited more potential antibacterial activity than the Zr(IV) complex against all the tested pathogens.
References (5)
- 1 New developments in the chemistry of peroxo-metal and chromium(VI)-oxidant systems [DOI]
- 2 Reaction aspects of peroxo copper complexes relevant to copper containing monooxygenases. [DOI]
- 3 Metal ion activation of dioxygen
- 4 Peroxo complexes of zirconium(IV), thorium(IV), molybdenum(VI), tungsten(VI) and uranium(VI) containing two quadridentate onno Schiff bases [DOI]
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