Synthesis and Characterization of Bisdithiocarbamates from Weak Nitrogen Bases and Its Metal Complexes
Shuchi Tiwari, K. V. Reddy, Anjali Bajpai, Kanchan Khare, V. Nagaraju
International Research Journal of Pure and Applied Chemistry · pp. 78–91 · Published 12 Mar 2015
10.9734/IRJPAC/2015/6588Abstract
In the present study, disodium salts of bisdithiocarbamates have been prepared from urea, thiourea, dithiooxamide and 1,3-diaminopropanewith carbon disulfide under strong alkaline medium of a sodium hydroxide solution. All ligands possessed good chelating ability for various metal ions. Metal complexes of urea bisdithiocarbamates was synthesized with Co (II), Ni (II), Zn (II), and Pb(II). The nature of metal complexes was amorphous and solid. The prepared ligands and complexes were characterized by elemental analysis, electronic, infrared (IR) spectroscopy, conductivity measurements, magnetic measurements and thermogravimetric analysis (TGA). Electronic spectra and magnetic measurements indicate that the complexes have contained octahedral geometry.
Cited by 0
No indexed citations yet.
Related research
- Thermal Decomposition of Camel Grass and Lemon Grass — shares topic coverage
Article metrics
Real usage data collected on this platform.
0
Page views
0
PDF downloads
0
Outbound clicks
0
Citations
Views by country
Approximate, from request IP at view time — not citizenship or institution. Countries with fewer than 5 views are grouped as "Other".
No views recorded yet.
Traffic sources
Referring site, by host.
No traffic recorded yet.
Views and downloads exclude known bots/crawlers. Citations combines this platform's own DOI-resolved index with each external source's own reported total — see Cited by above for individually listed citing works. Last refreshed 0 seconds ago.