Polyvinyl Butyral Synthesis Process Based on Deep Eutectic Solvent as a Catalyst
Po Li, Weilan Xue, Zuoxiang Zeng, Li Sun, Yu Bai
Asian Journal of Chemical Sciences · pp. 31–39 · Published 27 Sep 2021
10.9734/ajocs/2021/v10i319095Abstract
Polyvinyl butyral (PVB) was prepared by the condensation reaction of polyvinyl alcohol (PVA) with n-butyraldehyde using a catalyst which is a kind of deep eutectic solvent (DES) made of dodecyltrimethylammonium chloride and p-toluenesulfonic acid. The raw materials and products were characterized by Fourier transform infrared spectroscopy (FT-IR). The effects of the following reaction conditions on the degree of PVB acetal, yield and agglomeration of the products were investigated: the mass ratio of n-butyraldehyde to PVA (mBA/mPVA) of 0.48-0.96, the mass ratio of catalyst to PVA (mcat/mPVA) of 0.16-0.64, the low temperature reaction temperature (5-20℃), and the low temperature reaction time (1-3h). The results showed that at mBA/mPVA =0.8, mcat/mPVA =0.32, low temperature reaction temperature of 15°C and low temperature reaction time of 2 hours, the obtained PVB was a homogeneous powder with the highest acetal degree of 73.85%.
Cited by 3
R. M. Omer, Ahmed S. Ahmed, K. K. Ibraheem · Results in Engineering · 2026
Tongming Xu, Haiming Zhang, Bo-Zhao Li · Journal of Chemical Engineering of Japan · 2025
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