G. C. Nwanisiobi

Iodine Volatilisation and Analyte Loss in Vegetable Sample Preparation: A Comparative Evaluation of Microwave Digestion, Dry Ashing, and Alkaline Extraction

C. J. O. Anarado, N. E. Ogua, G. C. Nwanisiobi & C. E. Anarado · Chemical Science International Journal · 2026

Accurate determination of iodine in vegetable matrices depends strongly on sample preparation because iodine can be lost through volatilisation under unsuitable digestion conditions. This review evaluates iodine volatilisation and analyte loss during three commonly used preparati...